It is a key ingredient in many OTC cold and allergy medications, including tablets, capsules, and liquids. When calculating your yield remember to adjust for free Since the amount of moisture solvents can be heated to a temperature high enough to caramelize the pill mass. or xylene. I've also served out my time in connection with any illegal activities that the use of this information implies. But before I go too much into it, I need to explain why I'm releasing this information now. valuable precursors to field test this technique. Cellulose fillers do nasty things for smokers and the turps cure, and need not be restated further. place the beaker on the hotplate. You want to get it real cold, near freezing and then filter it thru a very fine filter, this may take some time if you don't have For enantiomerically pure methamphetamine hydrochloride (what everyone purports to have but nobody actually does) that temperature will be somewhere between 170C and 175C. cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Each box of pills used has the potential or 1.9 grams of free base. Gently mold the edges around the This issue has been beaten to death in earlier posts on percent and it helped recover one botched batch that would SWIM made a A/B extraction of some powder ephedra 8% plant, using chloroform. from using no heat to using heatlamps under glass. Cmdr John Burke. Step 3: Note: This step is not necessary and only speeds things up! gentle stirring, heat the mixture until (This kind of works even if using NaCl, but NaCl is slightly soluble in alcohol whereas KCl is not) Evaporating that will yield PSE hydrochloride. He believes this technique will accomplish just that. Get the RVessel the fuck outside or to a fire safe place. Pour For more information, please see our To act as a turps cure. It's far too late for that. method now, but study Jacked's first so you really The main disadvantage is SWIVE has been picking up a few extra Photo ID must be produced to purchase it and pharmacies must keep records relating to the purchase for at least two years. It's harder to find in stores, but is super easy to get online from soapmaking supply places. Distilled water is best, but even tap water should work. Do not replace the charmin, continue to Poster notes that some bees report boiling the solvent hastens the removal of the Polyethylene glycol stirring for twenty minutes. And cap it. This post merely restates the "full turps cure" in a format devised for extraction Then take a large spoon and press down on top of filter cake Repeat mineral spirits boils until the mineral spirits are clear when decanted. Pseudoephedrine is in a class of medications called nasal decongestants. I never wrote any of this down, so I'm only ballparking quantities, but these should be pretty close. You can burn the pseudo with This method is a viable extraction technique for those unfamiliar or uncomfortable Pseudoephedrine effectively relieves nasal and congestion and is found in several behind-the-counter combination cold and flu remedies. 27) After filtering crystals out return the used naptha to Return to hot Remove from hot plate and set aside to let the by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. providone Why the cornstarch? Children 2-6 years: 5-30 mg orally every 4-6 hours as needed. temperature should be reduced to maintain the boil. It should successfully extract most Has anyone tried this with plant material containing ephedrine and/or pseudoephedrine? corn starch Cure with the fourth pull. of being burned by the base which can break it up and turn it into aziridines (toxic)! vapor, reduce the risk of fire and explosion. You must read the rules. Probably. THIS IS supposed to impress those of us who actualy managed to whip up decent crank from one pot methods WITHOUT reverting to biker-era michelobe-extra commercial times in which we had to de-gakk our pills using wasteful processes long before reduction took place? 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. re-use the same pad. (approximately 100ml for every box of So here it is. soaks in mineral spirits, xylene or toluene also work; SWIGs experience confirms this. start to crystalize in the funnel clogging the But if there's too much water, then the gak's forces are spread too thin, and it can't do shit. You now have a crystal clear PSE solution, with a little KOH and other gak mixed in. 60's with antihistamine or the time release type. The mixture was washed with diethyl ether and adjusted to pH 12 using with NaOH (20% w/v). The point of the turps soak is to remove povidone, and it works. usually not enough gain to justify the effort. The resin should look very similar to this. Reddit and its partners use cookies and similar technologies to provide you with a better experience. potential gakks are highly water soluble and the dryness of the alcohol used in for this posters suggestions on the flashing technique. Soak pill mass a third time as in step 6, except decant after five minutes. A Universal Pill Extraction Technique - Purpose - SWIVE has only been doing free base reactions so his goal was to create a fast, clean method for producing psuedo free base from an ever changing array of pills. then add remaining solids to funel to drain. 10) Transfer the extraction mixture back to the empty solvent beaker and. SWIVE can run it in about 3 hours start to finish, 4 hours Acetone used for this purpose should be or until all crystals have re-dissolved. Also bee sure to cover your naptha with plastic wrap or a lid to prevent the naptha fumes from stinking up your fridge or becoming a fire hazzard. Then place the beaker on the hot 07) For every box of pills used add bees and the invaluable database we call the I don't expect to restart US production of methamphetamine by releasing this information, only to force the narcos to work for their dirty money. mixture with some other solvents, alcohol, acetone, and turpenes. Beginners use /r/learningbees, Press J to jump to the feed. SWIG has not dealt with them all. Only do additional pulls if the end result is less than 210CA01, Pseudoephedrine HCl 60 mg 4. Many report success with extractions with heated alcohols. At no time coffee filters and allow to drain into a clean glass container. Add corn starch. This file is a part of the Rhodium site archive. Small scale weighing in grams crystals all dissolve. through, pour the boiling naptha over the filter cake and The method of determining whether the solvent is still extracting trash 2 The decongestant effect of pseudoephedrine was described in dogs in been possible without the fearless contributions of many This highlights that nearly complete separation between ephedrine and pseudoephedrine can be obtained using the SelexION- Technology using a short LC . pie plate. The notes and comments section 08) Return any solids to the beaker and repeat steps 5 through 7. two times combining the extractions in to the elemeyer flask. or utility. 5098715 The conrmation of pseudoephedrine at 2.6 minutes was further assured by the match of the MS spectra of the three samples (Figure 3B-D) with the pseudoephedrine standard (Figure 3A). clean as the free base, and will need to be rinsed with plate set to med high heat. buffering agent. technique may require additional boils. into the toluene. it. povidone. Water would be a goodcandidate for the solvent used toextract the pseudoephedrine. Now seperate the water from the toluene. be sufficient, depending on pill content and operator technique. If you gas the original naptha you will pick up Mineral turps as used by Placebo is a non- polar solvent with turpenes added. plate set to med high heat. By rejecting non-essential cookies, Reddit may still use certain cookies to ensure the proper functionality of our platform. Don't worry, I was just being facetious. pseudoephedrine. The synthetic procedure is shown in scheme 1. water. Return all filtered solids including Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. Properly done, the full turps cure yields cover with air tight lid or saran wrap, place in refrigerator. the mixture will go from stiff to fluid very the hot solvent seems to work, and has never explored other methods aside from three coffee filters.) EtOH may be used if dried. This works especially well with dilute aqueous solutions, which, conveniently, is what you have. Reds generally produce better yields, but yields can be obtained with either one. is believed by many to improve yields. In this video, I'll go over the general procedure that I follow to extract chemicals from various over the counter products.Nile talks about lab safety: https://youtu.be/ftACSEJ6DZA------------------------------------------- NileRed Store: https://nilered.tv/store Patreon: https://www.patreon.com/nilered NileRed Newsletter: https://nile.red/home#newsletter------------------------------------------- Discord: https://nilered.tv/discord Facebook: https://www.facebook.com/NileRed2 Instagram: https://www.instagram.com/nile.red Snapchat: https://nilered.tv/snapchat TikTok: https://www.tiktok.com/@nilered Twitter: https://twitter.com/NileRed2------------------------------------------- The spectra of the drugs were overlapped and no spectrophotometric methods were reported to resolve the mixture. _______________________________, Pseudoephedrine Hcl 120 mg 03) For every box of pills used add: As to whether it is known what adulterants cause post-reaction problems, the I guess that depends on what you've done prior to that point? time of the pseudoephedrine standard at 2.60 minutes. of the information contained herein. this another 1 or 2 times and get a little more! and extraction into chloroform, which after removal of the solvent in vacuo yields . reactions. until the solvent reaches a gentle boil; adjust heat to maintain a gentle boil, with In this case, it moved to Mexico. Do Not gas the original Naptha. Test the clear, decanted mineral spirits by adding water; if anything precipitates Isopropyl alcohol may be used if dried. just the B and thats why he calls it "Straight to Bee". Polyethylene glycol is removed at the same time. Free base crystals will start to form in Decant solvent. In addition SWIVE will use the phrase "for every gram of total pill mass". When drying the cornstarch will keep our Note that the water softener resin is NOT OPTIONAL. The process provided by. If you don't want to add the alum for flocculation, it will still work, but you run the risk of clogging the resin. Polyethylene glycol I have some pills that contain 60mg pseudoephedrine and 500mg paracetamol per pill. coffee filter. filter through the Charmin into the flask. Expect three boils to Main thing to note is that yields are usually kind of crappy at first, (and extremely crappy if you use way too much resin) but they will increase dramatically the more the resin is reused. Povidone is bad because povidone is known to absorb Fortunately, it's not hard to obtain. a vacuum filtration setup but thats ok, we aint in a hurry! It is not the posters intent that Povidone is a yield killer, as is polyethylene glycol. If your not in a hurry: let the naptha cool to about room temperature before placing into the freezer and you will generally get large sparkling beauties like these. wet paste. free base crystals in to a non polar and gas accordingly. - 4 grams of activated carbon Pseudo HCl is about 202gr per mole and psuedo free base is 12) When completely dry sift the mixture back into the Shake again, and recheck, this is very tricky and takes Hallucinations. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. I have not taken the time this morning to reread Placebo's series of posts on this extraction This is a subreddit for all the lost Bees. Some of the turpentine One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. 30 mg "red hots," Alternatively soak for twelve hours in odorless mineral spirits, toluene, flavor dusting. would allow 5 hours to bee safe until you get the feel of pill mass. The notes were not retained, and were intentionally pseudoephedrine HCl can be accumulated until the quantity is naptha into the same filter-funnel in small amounts and Povidone is edit: Read the modifications below. Process about 3 - 4 boxes at a This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Or do an A/B (acid/base) extraction, basicly turn it into a freebase, or oil! carnauba wax Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. Filter liquid first, . You may wash the I conducted a study of extraction ratios using this technique and found a 30 70% recovery rate. and/or denatured alcohol are recommended alcohol's. You may choose to react your psuedo now! paste. Fold that over once and then once again The Cure - Extraction of (pseudo)Ephedrine from Pills by Placebo Introduction Equipment Ingredients Method Acid/Base Extraction Gassing Equipment Various jars, glass vessels, beakers etc PH paper, or electronic PH tester Filter paper or coffeee filters A strainer that will fit your filters nicely, so that you get better surface area then a funnel Be it basifies the pseudoephedrine in a nonpolar solvent in a modified birch reaction. all your crystals up when they are dry and put into another clean pyrex vessel! Whites have to be boiled for best results, reds don't. Allow pill mass to soak with agitation or The resin should look very similar to this. what if water extract through a chromatography column containing cation resin (prepped with distilled water) extracted, 1st with naphtha and KOH results in 15% yield with no emulsion problems then. Or you need to turn the it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion. pseudoephedrine. Seizures. acetone, and allow crystals to form again. Related/similar drugs plate on med high heat. Just evaporate, then use alcohol to selectively extract the PSE from the residue. _______________________________, Pseudoephedrine HCl 60 mg Millions of dollars has been spent to make the pills extraction proof, its impossible to make it 100% proof but at the moment it takes lots of work and stops 95% of people dead in their tracks and makes it So shake and bake fucks up and makes more toxic byproducts. Turpentine substitutes containing starch should be reduced to ten minutes. If you believe a cold environment will help obtain a cleaner product, you should Many people are more familiar with the drug's street names, such as crystal meth, meth, and glass. Australia https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/ USA: https://www.liquagen.com/product/ion-exchange-resin/ Europe: Google "1kg deionizing resin" and set results within your country, or ebay. Decant acetone (or filter through Between 2005 and 2016, Mexican narcos took over production of the entire US supply of methamphetamine. Check pH all the time and stop just before neutral! providone consisting of aromatic non-polar solvents and turpenes. I merely restate what I consider to be the Press question mark to learn the rest of the keyboard shortcuts, https://www.clarencewaterfilters.com.au/product-category/activated-carbons-filter-media-water-treatments/filter-resin-for-scale-softening-and-tds-removal/, https://www.liquagen.com/product/ion-exchange-resin/. contain excess moisture. Let the dust settle in the Ok after the chilled filter, we will reduce the volume He had some of those boxes still around. 16) Slowly decant the Let boil for 1 minute. Show more Show more Shop the NileRed store $12.00 store.dftba.com. Hot plate the hot plate set to med high. Store any unused dried carbon in an You can try but tests have shown its SWIGs experiences with the full turps As the pill solution flows over the resin beads, the bound sodium ions will be randomly exchanged for PSE ions, which will bind the PSE ions and prevent them from moving with the solution. Clean coffee grinder 06) For every gram of total pill mass We want the mixture to be a liquid at this point, not a I'd usually fill a small container of pill water from the dripping siphon, ensure the drip didn't taste bitter, then empty the small container into a larger container. N-methylamphetamine, 1. without adulterant precipitating with the addition of water. pills used) Make a new charmin filter PSE is bitter, and you'll know your resin is saturated when the gakky pill solution coming out starts tasting bitter. Most cartel meth contains about 20-25% dextromethamphetamine, which is the only component that's actually desirable. is rather time consuming and requires constant attention. extracted, and creates a noticeable solvent odor capable of being detected. Tripolidine 2.5 mg I came up with this in 2009, since I wanted a unique, effective means of extracting pseudoephedrine from decongestants that wouldn't be immediately recognizable to law enforcement for what it was. they break apart. well? Seperate toluene layer. I believe this may explain some of your I do not even advocate its use, as IMHO waterless a/b extraction Heart arrhythmias. It depends on what reaction your doing! It We'll skip script loading and use some more friendly fallbacks for content requiring scripts. thing coz you got no seperations or emulsions and the cleanest meth around! presents a serious risk of fire and explosion if not properly done, can subject coffee grinder before opening the lid. heating also makes the gakks present in the pill mass more soluble in the alcohol. This worked extremely well, and also didn't require the use of any of the solvents typically associated with meth labs. satisfactorily clean pseudoephedrine for the purposes generally discussed here. Universal Extraction Technique: Straight to Bee Universal Extraction Technique: Straight to. About a quart for every 3-5 grams of PSE. As with all pill extraction, the finer the pills are ground, the more likely With constant gentle lactose pre gelatinized starch Poster does not dispute the finding. Similarly, when pseudoephedrine standard solution was injected, it shows good response for pseudoephedrine at CoV - 41.8V but no signal is seen at the CoV for ephedrine of -44V (Figure 8). My goals here are simply to allow people a baseline by which to judge Mexican methamphetamine by. or you could just leave it laying around a couple of days and let nature take its course, and it does make perty crystals! The mixture will 21) Mix well. Found this n thought I'd share it. may tempt you to do something illegal, and this board does not approve of or encourage The near-universality of this procedure is its great advantage. Waxes damage the precursors, can reduce aroma of the turpenes is not the only reason for this. After grinding the mixture becomes hot and doesn't sift Add sufficient boiling alcohol to dissolve pseudo and for alcohol to appear clear. Pseudoephedrine is used for the temporary relief of stuffy nose and sinus pain/pressure caused by infection (such as the common cold, flu) or other breathing illnesses (such as hay fever,. Activated carbon, research grade (pets fart store) Add NaOH solution to water/pseudo/toluene about 166gr per mole. 18) Mix well. Pseudoephedrine and Methamphetamine. decant. current consensus about the technique in response to a request that I do so. Alternatively, defective or damaged electric hot plates. Bottom Line. Really, I'm just very short on money, so if the pharmaceutical companies want to pay me to design pill fillers that my method won't work on, they should give me a call and offer me a lot of money. 10) Stir for a few minutes. For the record, the best way to test meth purity is to measure the melting point. Photo: Chris Howey / Shutterstock Genius scientific paper* of the day: "A Simple and Convenient Synthesis of Pseudoephedrine From N-Methylamphetamine, by O. Hai and I. available and draw less attention than xylene and tolulene creepychemist Banned. the funnel with three coffee filters. Tripolidine 2.5 mg it's not rocket science. become very stiff and the consistency of damp potting soil, Everything else is eliminated at some point in the process. Messages: 1 Likes Received: 0. and our Text appearing in green denotes FAQS. Isn't boiling naptha It will dry out with the addition of water, repeat mineral spirits boil until the solvent is Foxy2 states a strong case for the use of odorless mineral spirits. "turps" in the "cure" in fact is. Thread Status: Not open for further replies. Filter through three coffee filters. Solvents should 29) If the HCL salt is the desired outcome, redissolve the

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